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semi preparative hplc separation  (YMC America)


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    YMC America semi preparative hplc separation
    Semi Preparative Hplc Separation, supplied by YMC America, used in various techniques. Bioz Stars score: 96/100, based on 1595 PubMed citations. ZERO BIAS - scores, article reviews, protocol conditions and more
    https://www.bioz.com/product/semi+preparative+hplc+separation/pm31461283__ja9b06592_si_001-183-40-44?v=YMC+America
    Average 96 stars, based on 1595 article reviews
    semi preparative hplc separation - by Bioz Stars, 2026-08
    96/100 stars

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    Figure 3. (A) Semi-preparative radio- and UV-HPLC chromatograms of [18F]BIT1 (conditions: Reprosil-Pur C18-AQ, 250 × 10 mm, 46% MeCN/20 mM NH4OAcaq., 5.5 mL/min); (B) Analytical radio- and UV-HPLC chromatograms of the final product of [18F]BIT1 spiked with the non-radioactive reference BIT1 (conditions: Reprosil-Pur C18-AQ, 250 × 4.6 mm, gradient system with eluent mixture of MeCN/20 mM NH4OAcaq., 1.0 mL/min).

    Journal: Molecules

    Article Title: Radiosynthesis and Biological Investigation of a Novel Fluorine-18 Labeled Benzoimidazotriazine- Based Radioligand for the Imaging of Phosphodiesterase 2A with Positron Emission Tomography

    doi: 10.3390/molecules24224149

    Figure Lengend Snippet: Figure 3. (A) Semi-preparative radio- and UV-HPLC chromatograms of [18F]BIT1 (conditions: Reprosil-Pur C18-AQ, 250 × 10 mm, 46% MeCN/20 mM NH4OAcaq., 5.5 mL/min); (B) Analytical radio- and UV-HPLC chromatograms of the final product of [18F]BIT1 spiked with the non-radioactive reference BIT1 (conditions: Reprosil-Pur C18-AQ, 250 × 4.6 mm, gradient system with eluent mixture of MeCN/20 mM NH4OAcaq., 1.0 mL/min).

    Article Snippet: The semi-preparative HPLC separations in the manual radiosynthesis were performed on a JASCO LC-2000 system, using a PU-2080-20 pump, an UV/VIS-2075 detector coupled with a radioactivity HPLC flow monitor (Gabi Star, raytest Isotopenmessgeräte GmbH, Straubenhardt, Germany) and a fraction collector (Advantec CHF-122SC, Dublin, CA, USA).

    Techniques:

    Figure 5. Representative analytical HPLC chromatogram: (A) plasma and (B) brain samples at 30 min p.i of [18F]BIT1 in a CD-1 mouse; (C) sample from incubation of BIT1 with mouse liver microsomes (MLM) in the presence of NADPH for 90 min at 37 ◦C (UV detection: 228 nm; axis of retention time was adjusted). Conditions: isocratic system, column: Reprosil-Pur C18-AQ, 250 × 4.6 mm; eluent: 42% MeCN in 20 mM NH4OAcaq., flow: 1.0 mL/min.

    Journal: Molecules

    Article Title: Radiosynthesis and Biological Investigation of a Novel Fluorine-18 Labeled Benzoimidazotriazine- Based Radioligand for the Imaging of Phosphodiesterase 2A with Positron Emission Tomography

    doi: 10.3390/molecules24224149

    Figure Lengend Snippet: Figure 5. Representative analytical HPLC chromatogram: (A) plasma and (B) brain samples at 30 min p.i of [18F]BIT1 in a CD-1 mouse; (C) sample from incubation of BIT1 with mouse liver microsomes (MLM) in the presence of NADPH for 90 min at 37 ◦C (UV detection: 228 nm; axis of retention time was adjusted). Conditions: isocratic system, column: Reprosil-Pur C18-AQ, 250 × 4.6 mm; eluent: 42% MeCN in 20 mM NH4OAcaq., flow: 1.0 mL/min.

    Article Snippet: The semi-preparative HPLC separations in the manual radiosynthesis were performed on a JASCO LC-2000 system, using a PU-2080-20 pump, an UV/VIS-2075 detector coupled with a radioactivity HPLC flow monitor (Gabi Star, raytest Isotopenmessgeräte GmbH, Straubenhardt, Germany) and a fraction collector (Advantec CHF-122SC, Dublin, CA, USA).

    Techniques: Clinical Proteomics, Incubation